Type HP D 5 (FCT Systeme GmbH)
Pressing force | 3 - 50 kN |
Max. diameter of a graphite mould | 30 mm |
Operating temperature | up to 2200°C |
Atmosphere | vacuum or argon |
Heating modes | continuous/pulse |
Planetary mill Pulverisette 7 (Fritsch) |
Planetary mill PM 400 (Retsch) |
|
rotary speed | to 1000 rev/min | to 400 rev/min |
Cryogenic ball mill CryoMill (Retsch) | |
Frequency | 3-25 Hz |
milling at a temperature of liquid nitrogen |
Analysis of grain size distribution by X-ray diffraction technique | |
Dry measurement within a range of | 0,1 – 2000 µm |
Wet measurement within a range of | 0,01 – 2000 µm |
Possibility of using different disperging liquids, e.g. water, glycol, glycerine |
Identification of phase composition based on PDF-2 catalogue data from ICDD |
Texture determination from pole figures and inverse plot figures |
Measurements of the size of crystallites and stresses based on a profile and position of the X-ray diffraction lines |
Quantitative and qualitative analysis in micro-areas by energy-dispersive (EDS) technique and wavelength dispersive(WDS) analysis with particular account of light elements, |
Detection limits:
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Surface analysis, X-ray elements distribution maps, linear analysis including examination of a matrix, inclusions and microstructural discontinuities, |
Microstructure analysis by EBSD, technique including determination of orientation of particular grains and their size. |
Measurements of electric resistance by | the dc four-terminal method, measurement of thermoelectric power (Seebeck coefficient) |
Temperature range | from - 100°C to 1100°C |
Measurement of thermoelectric power |